Theory: Specific gravity is defined as the ratio between weight of a given volume of material and weight of an equal volume of water. In case of cement, specific gravity is determined by use of a Le Chatelier’s flask (Figure Below). Sometimes, a specific gravity bottle may be employed to a standard Le Chatelier’s flask. To determine the specific gravity of cement, kerosene is used which does not react with cement. The specific gravity of OPC is generally around 3.15.
Le Chaterliers flask |
Objective: Determination of specific gravity of cement using Le-Chatelier flash.
Reference: IS 4031
(Part-11):1988.
Apparatus: Le Chaterliers
flask, weighing balance, kerosene (free from water).
Material: Ordinary
Portland cement; Water; Grease
Procedure:
1. Dry the flask carefully and
fill with kerosene or naphtha to a point on the stem
2. Record the level of the liquid
in the flask as initial reading.
3. Put a weighted quantity of
cement (about 60 g) into the flask so that level of
4. After putting all the cement
to the flask, roll the flask gently in an inclined
5. Note down the new liquid level
as final reading.
Observations:
• Weight of cement
used in g. (W1) : _______
• Initial reading
of flask in ml (V1) : _______
• Final reading of
flask in ml (V2) : _______
• Volume of cement
particle (V2
- V1) : _______
• Weight of equal
volume of water in g. (W2) : _______
• Specific gravity
of cement (W1/ W2) : _______
Result and
conclusion:
Precautions: (Discuss
about the precautions to be taken while conducting this experiment)
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